General Information and Rules for 5.35 Introduction to Experimental Chemistry
General Information and Rules (PDF)
Module 1: Fundamentals of Spectroscopy
Module 1 Experimental Procedures (PDF - 1.7MB)
| WEEK # | TOPICS | ACCOMPANYING FILES |
|---|---|---|
| 1 | Introduction to Electronic Spectroscopy (Experiments 2–4) | PreLab 1: UV-Vis (PDF) |
| 2 | IR Spectroscopy (Experiments 5–6) | PreLab 2: IR Spectroscopy (PDF) |
| 3 | IR Spectroscopy of Proteins (Experiment 7) | PreLab 3: IR Spectroscopy of Proteins (PDF) |
| 4 | TeachSpin 15 MHz NMR (Experiment 8) | PreLab 4: 15 MHz NMR (PDF) |
| 5 | NMR, 300 MHz (Experiment 9) | PreLab 5: 300 MHz NMR (PDF) |
| 6 | Oral Examinations | Oral Exam Rubric (PDF) |
Module 2: Synthesis of Coordination Compounds and Kinetics
Module 2 Experimental Procedures (PDF)
| WEEK # | TOPICS | ACCOMPANYING FILES |
|---|---|---|
| 7 | Synthesis of [Co(NNH3)4(CO3)]NO3 | PreLab 1 (PDF) |
| 2 | Synthesis of [Co(NNH3)5Cl]Cl2 | PreLab 2 (PDF) |
| 9 | Lambert-Beer study | PreLab 3 (PDF) |
| 10 | Kinetics Measuremts at 60 C | PreLab 4 (PDF) |
| 11 | Kinetics Measuremts at 40 C | PreLab 5 (PDF) |
| 12 | Kinetics Measuremts at 70 C | PreLab 6 (PDF) |
| 13 | Report Interview | Written Report Guidelines (PDF) |